柠檬腈,无色至淡黄色液体,以柠檬醛为原料与羟胺生成柠檬醛肟,再用乙酐为脱水剂转化为柠檬腈。适于配制花香型和果香型化妆品和皂用香精,不宜食用。
本文对利用山苍子油中柠檬醛合成柠檬腈香料进行了新探和改进。
The synthesis of lemonile perfume from litsea cubeba oil is newly studied and re-formed.
从山苍子提取出的柠檬醛,与硫酸羟胺反应生成柠朦肟,脱水后可得到柠檬腈。
Lemonile was manufactured by the dehydration of citral oxime obtained by the reaction of hydroxylamine sulfuride and citral abstracted from litsea cubeba oil.
研究了不同碱对柠檬肟的催化脱水效果及不同PTC的催化作用效果,并用正交实验设计法确定了使用KOH- TBAB催化脱水法合成柠檬腈的最佳反应条件。
The catalytic dehydration of lemonile with various alkalis and PTC was studied. The optimal conditions dehydration to lemonile for KOH TBAB catalytic by orthogonal design were determined.
应用推荐