本文对利用山苍子油中柠檬醛合成柠檬腈香料进行了新探和改进。
The synthesis of lemonile perfume from litsea cubeba oil is newly studied and re-formed.
从山苍子提取出的柠檬醛,与硫酸羟胺反应生成柠朦肟,脱水后可得到柠檬腈。
Lemonile was manufactured by the dehydration of citral oxime obtained by the reaction of hydroxylamine sulfuride and citral abstracted from litsea cubeba oil.
研究了不同碱对柠檬肟的催化脱水效果及不同PTC的催化作用效果,并用正交实验设计法确定了使用KOH- TBAB催化脱水法合成柠檬腈的最佳反应条件。
The catalytic dehydration of lemonile with various alkalis and PTC was studied. The optimal conditions dehydration to lemonile for KOH TBAB catalytic by orthogonal design were determined.
本文提出了在乙腈- 乙醇-水混合溶剂中以柠檬酸钠作络合剂, 三氯化钛还原非水溶性偶氮染料和颜料。
Sodium citrate was used as a complex catalyst for the titanium trichloride to reduce insoluble azo dyes and pigments in acetonitrile-alcohol-water system.
本文提出了在乙腈- 乙醇-水混合溶剂中以柠檬酸钠作络合剂, 三氯化钛还原非水溶性偶氮染料和颜料。
Sodium citrate was used as a complex catalyst for the titanium trichloride to reduce insoluble azo dyes and pigments in acetonitrile-alcohol-water system.
应用推荐