The synthesis of lemonile perfume from litsea cubeba oil is newly studied and re-formed.
本文对利用山苍子油中柠檬醛合成柠檬腈香料进行了新探和改进。
Lemonile was manufactured by the dehydration of citral oxime obtained by the reaction of hydroxylamine sulfuride and citral abstracted from litsea cubeba oil.
从山苍子提取出的柠檬醛,与硫酸羟胺反应生成柠朦肟,脱水后可得到柠檬腈。
The catalytic dehydration of lemonile with various alkalis and PTC was studied. The optimal conditions dehydration to lemonile for KOH TBAB catalytic by orthogonal design were determined.
研究了不同碱对柠檬肟的催化脱水效果及不同PTC的催化作用效果,并用正交实验设计法确定了使用KOH- TBAB催化脱水法合成柠檬腈的最佳反应条件。
应用推荐