晶须产品经x -射线衍射鉴定为纯相。
The whisker product is identified to be pure phase by the X-ray diffraction.
通常的增量法X射线衍射定量相分析需用纯相作增量剂，条件苛刻。
The pure doping samples of single phase are necessary to the common doping methods in quantitative X-ray diffraction phase analysis.
详细研究结果如下：反应温度、硫源和混合溶剂体系是合成纯相二硫化镍微球的关键。
The results can be summarized as follows:Reaction temperature, sulfur source and volume ratio of the mixed solvent were crucial to synthesize the NiS2 microspheres.
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