熔盐法也称熔盐合成法。通常采用一种或数种低熔点的盐类作为反应介质,反应物在熔盐中有一定的溶解度,使得反应在原子级进行。反应结束后,采用合适的溶剂将盐类溶解,经过滤洗涤后即可得到合成产物。
1.4.1 熔盐法 熔盐法(Molten Salt Synthesis,MSS)是在较低的反应温度下和较短的 反应时间内制备各向异性粉体的简便方法。
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...据可以看出,在制得 Y5V 瓷粉的相 结构上,固相法正常生产的瓷粉(ST-PMN)含有少 量恶化介电性能的焦绿石相,熔盐法(MSS-PMN) 制得的瓷粉均为 100%的钙钛矿相。
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亚熔盐法 sub-molten salt method
性熔盐法 reactive flux method
顶部籽晶熔盐法 TSSG
熔盐法晶体生长 crystal growth from flux
熔盐生长法 molten-salt growth ; salt growth
熔盐电解法 fused salt electrolysis process ; fused salt electrolysis ; fused salt process ; melts electrolysis proc es
熔盐反应法 molten salt reaction
熔盐极谱法 fusedsaltpolarography
The CCTO nanorods were successfully prepared by molten salt method. Thediameters of the nanorods are about 50~80nm, and 100~250nm of length.
然后,通过改进熔盐法一步反应合成了CCTO纳米棒,纳米棒直径大约50~80nm,长度达到100~250nm。
参考来源 - 新型类钙钛矿高介电常数氧化物的制备与结构表征On the contrary, molten salt synthesis has the advantages in high efficiency, simple operation, little pollution and low power wasting.
相比之下,熔盐法具有转化率高,工艺简单,少污染,低能耗等优点。
参考来源 - 熔盐法制备无机纳米材料及其性能研究·2,447,543篇论文数据,部分数据来源于NoteExpress
介绍了一种新的无机材料粉体的制备方法—熔盐法,以及该方法的部分应用。
As a new kind of methods to prepare inorganic material powders, molten salt method (MSM) and some of its applications are recommended in this paper.
采用熔盐法生长了一系列磷酸氧钛锡钾单晶体并测定了其晶体结构和相应的物理性质。
Single crystals of KTi 1- x Sn x OPO 4 solid solutions and KSnOPO 4 were grown by using flux method, and their structure and physical properties were studied.
反应性熔盐法的反应结果与多种因素有关,包括:反应物配比、反应温度、反应时间、升温速率、降温速率等。
The results of reactions are influenced by many factors, including reactant mole ratio, reaction temperature, heating program, and so on.
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