相比目前使用的水或甲醇溶剂纯化收率30%,发现以丙酮、乙酸、水的溶剂体系,精制更昔洛韦收率可显著提高到83.3%,高效液相色谱(HPLC)分析,产品纯度达到99.0%以上。
Ganciclovir could be purified to more than 99.0%(HPLC) by a combination of acetone, acetic acid and water in 83.3% recovery as compared with 30% one when using water or methanol as solvent.
方法用高效液相色谱(hplc)法考察疏肝理脾片主要指标成分芍药苷在原生产各环节中(水提液、精制液、干燥品等样品)的提取率、损失率、转移率。
Methods To explore the influences of each links of productive process on the rate of extraction, percentage loss and the transferring rate of paeoniflorin by HPLC.
从氟代甲苯出发,以醋酸为溶剂,采用液相空气氧化法,在钴锰盐和1,1,2,2-四溴乙烷催化体系存在下,合成了氟代苯甲酸,采用升华方法进行精制。
Fluorobenzoic acids were prepared from fluorotoluenes through liquid phase air oxidation with acetic acid as solvent and Co~(2+)-Mn~(2+)-1, 1,2,2-tetrabromoethane as catalyst.
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