将新戊酰氯氯化为制得的3-氯新戊酰氯在全回流的填充蒸馏塔中进行。
The chlorination of pivaloyl chloride to prepared 3-chloropivaloyl chloride was took place in a packed distillation column with total reflux.
方法：用氯仿作溶剂，在浴温条件下，4 羟甲基笼状双环磷酸酯分别与戊酰氯、己酰氯发生酰化反应。
Methods:Chloroform being solvent, under bath heat, 4 hydroxymethyl caged bicyclic phosphate acylated with pentanoyl chloride and hexanoyl chloride dividedly.
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