方法利用反相层析的方法进行分离纯化,根据化合物的化学性质与光谱数据鉴定其结构。
Methods to isolate the constituents by reverse phase chromatography, and characterize their structures by the analysis of chemical property and spectral data.
方法利用正相、反相硅胶柱和大孔树脂柱色谱分离,并通过波谱技术进行结构鉴定。
Methods The compounds were isolated by silica gel, ODS, and macroporous resin column chromatography and their structures were determined by means of spectral analysis.
方法采用硅胶和反相硅胶RP- 18柱色谱分离,运用有机波谱分析确定化合物结构。
Methods Three compounds were isolated by a combination of RP-18and silica gel column chromatographies, and their structures were identified by spectral methods.
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