要熟悉和矫捷运用仪器的相关操作屏(界面) 如:用反应过程监测(Reaction Monitor),不雅察反应时间进程曲线;用校准追踪(Calibration Trace)回首分析校准曲线;利用计数(Statistics)了解不同日子段病人测定均值及数...
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为达到此目的，监测原材料的质量和调整反应过程中硅铜触体是必需的。
For attaining this it was necessary that monitoring rial quality and adjusting to silicon-copper mass in the reaction process.
采用HPLC对反应过程进行监测，用光谱分析法鉴定产物结构。
The process of reaction was monitored by using HPLC. The product structure was analyzed by spectroscopic technique.
目前，合成过程的中间监测方法主要集中在胺酰化及脱保护反应，而对于中间体一活化酯的反应进程没有监测方法。
Currently, the reaction progress monitoring focuses on amide acylation and deprotection reaction, while there is no method for the reaction progress of the intermediate-active esters.
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