The experimental instrument, sample preparation and determination method of the trace element Se in solution by total reflection X-ray fluorescence analysis are described in this paper.
本文叙述了用全反射X荧光分析方法测定溶液中微量硒的实验装置、制样技术和测定方法。
All of them have been characterized by elementary analysis, NMR, IR and melting point determination, Among them, 10, 11 have been characterized by single-crystal X-ray analysis.
所得配合物均通过了元素分析、核磁、红外、熔点测定等进行了表征，其中10和11经过了X -单晶衍射的表征。
Rigaku 3080e3 X-ray spectrometer was applied to the determination of major and trace mineral elements in muskmelon, calibration was made by using national plant standard reference materials.
报道了日本理学3080e3型x -射线荧光光谱仪在测定甜瓜样品常量和微量矿质元素中的应用。
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