Ethyl pyruvate was synthesized from ethyl lactate using TBHP as oxidant and TBAB as phase transfer catalyst, the purity of product was over 98 %.
以叔丁基过氧化氢(TBHP)为氧化剂,四丁基溴化铵(TBAB)为相转移催化剂,有效地将乳酸乙酯氧化合成丙酮酸乙酯,产品纯度达98%以上。
The results show that the influences of solvent, reaction time, and molar ratio of styrene to catalyst or TBHP on the reaction is very important.
研究结果表明,反应温度、反应时间、溶剂种类、氧源用量和催化剂用量等反应条件对苯乙烯环氧化反应具有重要影响。
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