The structure of the target compound and the intermediates were confirmed by MS,1H-NMR and 13C-NMR. The total yield was 7.64% which was comparable with that in the literature.
结果与结论目标化合物和中间体的结构经MS、1H-NMR和13C-NMR确认,总收率为7.64%。
参考来源 - 肺动脉高压治疗药riociguat的合成·2,447,543篇论文数据,部分数据来源于NoteExpress
The target compound shows strong solvent effect in their SPEF spectra.
在不同极性溶剂中,化合物的荧光光谱表现出显著的溶剂效应。
RESULTS The target compound was obtained and purified yield was over 60%.
结果得到目标化合物,精品收率达60%以上。
The structure of target compound was confirmed by IR and elementary analysis.
产物经IR及元素分析表征了结构。
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