Moreover, higher water content in the ionic liquid was favorable for obtaining higher enantioselectivity, however it lowered the reaction rate and(DL)-menthol conversion.
另外,在离子液体中,水含量的增加在一定程度上可以增大酯化手性选择性,但反应速率会被降低。
Distilling excessive menthol after reaction, filtering the liquid phase at a high temperature, separating the catalyst, stewing the filtrate for overnight stratification.
反应后蒸馏出多余甲醇,反应液相趁热过滤,分离出催化剂,然后将滤液静置过夜分层。
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