Radix Scutellariae was examined by Silca gel-G, the mobile phase was ethyl acetate-butanone-formic acid-water (5:3:1:1).
黄芩:采用硅胶G板,以醋酸乙酯-丁酮-甲酸-水(5:3:1:1)为展开剂,显色剂为1%三氯化铁乙醇溶液。
Synthesis of coumarin-3-carboxylic acid through sodium ethoxide catalyzed synthesis of coumarin -3-carboxylic acid ethyl ester, followed by saponification, acidolysis cyclization was studied.
实验以水杨醛、丙二酸二乙酯为原料,乙醇钠为催化剂催化合成香豆素- 3 -羧酸乙酯,再经皂化、酸解环合合成香豆素- 3 -羧酸。
A simple TLC method for monitoring the synthetic process of 3-bromo-ethyl levulinate is reported, and the reaction condition is optimized.
用薄层色谱法监测溴素溴化乙酰丙酸乙酯生成3-溴乙酰丙酸乙酯的反应过程,优化了反应条件,方法简单,快速,准确。
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