Titanium nitride was synthesized by ammonia reduction and nitridation under flowing ammonia atmosphere while the content and tetragonal phase structure of zirconia was unchanged.
采用氨气还原氮化法，在流动的氨气氛下原位反应生成氮化钛，同时保持四方相氧化锆含量和结构不变。
The results show that the content of tetragonal phase is increasing in BNBT ceramics by direct reaction sintering method but still exhibiting a single phase of perovskite structure.
结果表明，直接反应烧结法不影响BNBT陶瓷的钙钛矿相结构，但可使准同型相界处组成的四方相含量增加；
The results of XRD and SEM show that the main crystal phase is the non-full-filled tetragonal tungsten bronze structure.
SEM结构分析可知，主晶相为非填满型钨青铜结构四方晶相。
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