香叶基砜的合成工艺改进 关键词: 香叶醇;香叶基砜;长链聚异戊二烯类化合物[gap=1053]Key words: geraniol; geranyl sulfone; polyisoprenoid compounds
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结果:两种条件下合成香叶基砜的收率均高于60%。
Results: The yield of geranyl sulfone could be higher than 60% under two conditions.
方法:以异丙醇或THF为溶剂,盐酸或硝酸为催化剂,香叶醇与苯亚磺酸钠回流反应18或28 h得香叶基砜。
Methods: In the presence of hydrochloric acid or nitric acid, geranyl sulfone was prepared from geraniol in isopropyl alcohol or THF under reflux conditions for 18 h or 28 h, respectively.
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