测量各杂质峰的面积和色谱图上除溶剂峰以外的总色谱峰面积,计算各杂质峰面积及其之和占总峰面积的百分率。由于峰面积归一化法误差较大。因此,通常用于粗略考察供试品中的杂质含量。除另外规定外,不宜用于微量杂质的检查。 英文:area normalization method
戊烷的定量则采用面积归一法。
方法水蒸气蒸馏法提取挥发油后,采用气相色谱-质谱法分析,用峰面积归一法测定成分的相对含量。
MethodsEssential oils were extracted from samples by steam distillation, The chemical constituents were determined by GC-MS with area normalization method.
用同一填充柱在程序升温条件下,分离轻苯及精制苯中各组份,并用直接面积归一法进行定量,苯系相对误差为0.94%。
The components of light benzene and purified benzene are separated using the same packed column in the condition of program raising temperature and quantified using direct area normal method.
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