1-氮杂-2-甲氧基-1-环庚烯的无溶剂合成 关键词： 己内酰胺; 硫酸二甲酯; 甲基化; 无溶剂合成[gap=663]Key words： caprolactam; dimethyl sulfate; methylation; solvent-free synthesis
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From the view of environmentally friendly, this thesis achieved the solvent-free synthesis of homoallyl and homopropargyl alcohols through zinc-mediated Barbier-Type reaction.
本论文从环境友好的角度出发,通过锌粉促进的Barbier-Type反应,实现了高烯丙基醇和高炔丙基醇的无溶剂合成。
参考来源 - 环境友好的Barbier类型反应研究·2,447,543篇论文数据，部分数据来源于NoteExpress
采用无溶剂法合成表面活性剂——棕榈酸葡甘聚糖酯（PKGM），并选择无毒复合溶剂进行分离、精制。
In the paper, surfactant palmitoylated konjac glucomannan(PKGM) was synthesized by solventless method and refined by non-toxic compounded solvent.
采用分子设计方法，将不饱和双键引入环氧树脂中合成了不饱和环氧树脂，并以苯乙烯为稀释剂制备了无溶剂型绝缘漆。
Unsaturated epoxy resins were synthesis by inducing vinyl into epoxy molecules via molecular design, and the solventless unsaturated epoxy insulating varnish was prepared with styrene as thinner.
对蔗糖脂肪酸酯的无溶剂法合成工艺进行改进，通过小试得到了较为理想的工艺参数，并在小试中加入了一种新的催化剂。
Improved the technics of synthesis on fatty acid sucrose esters by solventless method, and obtained better technics parameters by experiments. We added a new catalyst in the experiments.
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