The invention relates to a method to compounding 2-molindone that includes the following steps: using aniline as raw material, adding NaOH that the mol ratio is 1.0:2.0-1.0, adding solvent, taking reaction with chloroacetic chloride to form acylation material of aniline, and the mol ratio of chloroacetyl chloride is 2.0-1.0:1.0;
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The reaction conditions such as dosages of catalyst, 1, 4 dioxane and water, solvent type, reaction temperature and time, adding method were also studied.
同时还研究了催化剂用量、1,4二氧六环的用量、溶剂种类、反应温度、反应时间、水量及加水方式等对该反应的影响。
The spheroidicity zirconia is prepared by controlling the reactive temperatures, the precipitant reagents and adding additives through a alcohols solvent precipitation method.
采用醇溶剂沉淀法,通过控制温度、改变沉淀剂,加入添加剂等条件制备了椭球形氧化锆。
The effects of cyclohexanone and isoamyl alcohol on life of sealing solution and on inhibition of sealing flower, and the adding amount of organic solvent are also discussed.
探讨了环己酮和异戊醇对封闭液寿命的影响和对粉霜的抑制作用以及有机溶剂的添加量等问题。
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