论文:悲情与隐忍-中大网校论文网 关键词】 复方川乌止痛贴 酯型生物碱 总生物碱 [gap=810]Key words:Complex Prescription Monkshood Plaster; Ester-series alkaloid; Total alkaloid
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...,,,酯型生物碱 [gap=1105]Key words:Radix Aconiti Preparata; Process technology; Total alksloid; Alkloid of ester type ...
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...键词】 附子;总生物碱;酯型生物碱 [gap=1263]Key words: RALP(Radix aconiti lateralis preparata) ;TA(Total alkaloids) ; EA(Ester alkaloids) ...
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双酯型生物碱 Ester-alkaloids
Conclusion The content of ester alkaloids does not surpass 0.15 % in Radix Aconiti preparata, which conforms to the requirement of Chinese Pharmacopoeia.
结论制川乌中酯型生物碱含量均不超过0.15%,符合中国药典规定。
参考来源 - HPLC法测定不同地区制川乌中新乌头碱、次乌头碱及乌头碱的含量—《食品与药品·A版》—2008年第5期—龙源期刊网·2,447,543篇论文数据,部分数据来源于NoteExpress
结果在煎煮过程中双酯型生物碱溶解并发生水解反应 ,而脂类生物碱则难溶于水。
Results The results showed that the DDAs were solved and reduced by hydrolysis reaction, and the lipo-alkaloids were difficult to be soluted in the Decoction.
方法:采用酸性染料比色法测定附子总生物碱含量,反相高效液相色谱法测定双酯型生物碱含量,蒽酮-硫酸法测定多糖含量。
METHODS: The contents of total alkaloids, diester diterpenoid alkaloids and polysaccharides were measured by acid dye colorimetry, HPLC and sulphuric acid-anthrone colorimetric method respectively.
生川乌炮制后生物碱大多数由双酯型水解转化为单酯型,水解反应最容易发生的位置在C8位,水解反应的类型是烷氧键发生断裂的酯的碱性水解。
After processing of crude aconite roots, most of the diester diterpenoid alkaloids converted to the monoester form, while C8 was the major location for such reaction. It is a ty…
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