速灭辛乳油是由速灭威和辛硫磷复配而成，采用薄层分离，分别用碱解定胺法和溴化法对两种有效成分进行定量分析。
A quantitative analysis method-Thin layer chromatography-bromination-determine amine method was established for determining two active ingredients in the mixture of MTMC and phoxim.
用薄层色谱法监测溴素溴化乙酰丙酸乙酯生成3-溴乙酰丙酸乙酯的反应过程，优化了反应条件，方法简单，快速，准确。
A simple TLC method for monitoring the synthetic process of 3-bromo-ethyl levulinate is reported, and the reaction condition is optimized.
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