以壬基酚和三氯化磷为原料,芳烃为溶剂,采用直接酯化法,可制备三壬基苯基亚磷酸酯。
Antioxidant tris (nonyl phenyl) phosphate was prepared with nonyl phenol and phosphorus trichloride as raw materials, arene as solvent and by using directive esterification method.
方法:用氯仿作溶剂,在浴温条件下,4 羟甲基笼状双环磷酸酯分别与戊酰氯、己酰氯发生酰化反应。
Methods:Chloroform being solvent, under bath heat, 4 hydroxymethyl caged bicyclic phosphate acylated with pentanoyl chloride and hexanoyl chloride dividedly.
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