摘要目的：建立一种气相色谱法同时测定注射用青霉素钠中有机溶剂丁醇、乙酸乙酯、乙酸丁酯残留量的方法。
To found a method to detect the residual solvents of penicillin sodium for injection: butanol acetic ether and butyl acetate.
前言：目的：建立一种气相色谱法同时测定注射用青霉素钠中有机溶剂丁醇、乙酸乙酯、乙酸丁酯残留量的方法。
Objective: to found a method to detect the residual solvents of Penicillin Sodium for Injection: butanol, acetic ether and butyl acetate.
本文用生物样品与有机溶剂共沸蒸馏分离法对秦山核电厂附近秦山上松针中组织自由水氚进行测量。
Tissue Free Water(TFW)of pine needles is separated out through azeotropic distillation of pine needles and toluene, Recovery ratio of TFW is 90%.
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