建立了毛细管气相色谱法测定甲磺酸齐拉西酮中残留溶剂乙醇、异丙醇、二氯甲烷、正己烷、四氢呋喃、D MF、丙二酸二甲酯的残留量。
A capillary GC method with FID detector for the determination of residual organic solvents ethanol, isopropanol, dichloromethane, n-hexane, tetrahydrofuran, DMF and dimethyl malonate was established.
方法：以异丙醇或THF为溶剂，盐酸或硝酸为催化剂，香叶醇与苯亚磺酸钠回流反应18或28 h得香叶基砜。
Methods: In the presence of hydrochloric acid or nitric acid, geranyl sulfone was prepared from geraniol in isopropyl alcohol or THF under reflux conditions for 18 h or 28 h, respectively.
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