• 研究了稀碱催化下邻羟基苯乙酮甲醛在醇溶液中的羟醛缩合反应,溶剂可以循环使用,适合工业化生产

    During the condensation reaction, the feedstock remaining after reaction can be recycled, and this synthesis route was suitable for the commercial production.

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  • 前言2′,5′-二羟基苯乙酮和原甲酸缩合得到6- 羟基- 4- 色,再催化氢化得到标题化合物。

    6-Hydroxychroman was prepared by catalytic hydrogenation of 6-hydroxy-4-chromone, which was prepared via condensation of 2′, 5′-dihydroxyacetophenone with triethyl ortho-formate.

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  • 采用方法合成了鲜见文献报道的新化合物2 -羟基-3-氰甲基-5 -甲基乙酮方法具有反应时间、操作简便、收率等优点。

    Using the new method, 2 hydroxy 3 cyanmethyl 5 methyl acetophenone was synthesized in a short reaction period, and the yield was good.

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  • 羟基处于醛基邻位和对位甲醛与几种苯乙酮衍生物的缩合,多数没有得到预期的产物,收率极低;苯乙酮羟基对缩合反应影响很大羟基越多,缩合越困难。

    The groups in ring of benzaldehydes, no matter they are electron withdrowing or electron donating except of hydroxy, do not seem to have much effect on the yield.

    youdao

  • 羟基处于醛基邻位和对位甲醛与几种苯乙酮衍生物的缩合,多数没有得到预期的产物,收率极低;苯乙酮羟基对缩合反应影响很大羟基越多,缩合越困难。

    The groups in ring of benzaldehydes, no matter they are electron withdrowing or electron donating except of hydroxy, do not seem to have much effect on the yield.

    youdao

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