• 目的不同芳香进行环合缩合合成一系列的金酮。

    The objective is to cyclize and condense with different aromatic aldehydes to synthesize a series of aurones.

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  • 探讨了呋喃环合反应质子催化机理

    The mechanism was discussed in the proton acid catalytic reaction of furan phenol cyclization.

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  • 意思环合不上。

    What I mean is that the clasp cannot close.

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  • 所得公式适用于多个环合点的热环合反应

    These formulae derived can be used to the ring formation with multi-points ring formation reactions.

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  • 提出通过发掘节点间流水并行方法

    A new approach based on loop fusion is presented to exploit pipelining parallelism.

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  • 结果:所合成两个d成子光学纯度

    RESULTS: The two novel D ring synthons are of high optical purity.

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  • 方法肉桂为原料,酯化、氨化缩合-环合而得

    METHODS Cilnidipine was synthesized from cinnamyl alcohol by esterification, feminization and condensation - cyclization.

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  • 本文主要研究手性模板作用反应立体选择性

    The aim of this research is to study the stereoselectivity of photocyclization reaction in the act of chiral template.

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  • 发明采用氨基树脂环合技术合成卡贝缩宫素。

    The method adopts the amino resin to synthesize carbetocin by the solid phase cyclization technology.

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  • 然后再A成子偶联、关环、脱保护完成目标产物的全合成

    Then coupling with A ring synthon, closing, deprotection, the aim product was synthesized finally.

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  • 抵消成革至高无上舒适性提供了一个可定制适合

    Three offset hook-and-loop synthetic leather straps offer a customizable fit for supreme comfort.

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  • 报导杀鼠酮钠盐用途制备方法讨论了环合反应最佳条件

    In this article, the process and preparation of valone are reported. Moreover, its best condition of linking reaction was also discussed.

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  • 方法1,3-丙烷乙酰乙酸乙酯原料环合、开环、反应合成

    METHODS The compound was synthesized through the reaction of cyclization, split, bromination et al and using 1,3-propyl bromide and ethyl acetoacetate as raw materials.

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  • 氯乙酰巴比无水乙酸存在下环合不同芳香缩合合成噢类化合物

    In existence of the anhydrous sodium acetate using 5 chloroacetylbarbituric acid to cyclize and condense with different aromatic aldehydes to synthesize a series of aurones.

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  • 采用环合法合成虫啉具有产品纯度原料成本低等优点,是吡虫啉生产最佳工艺路线。

    The process so presented achieves merits of product with high purity and low cost in raw material.

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  • 环合反应条件缓和产品收率纯度高,在四氢咔唑类化合物的化学制备中具有重要参考价值。

    The conditions of reaction of cyclization were moderate, the purity and yield of the product was higher.

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  • 并且预测了四硫富瓦烯硫桥稠环合C_(60衍生物可能基态下产生长寿命电荷分离

    A long-lived charge-separated state may occur in the derivative of TTF-S-C_(60).

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  • 筛选2-丁酸起始原料氨解,酯化拆分环合五步反应得左乙拉西坦

    Screening for 2 - bromo- butyric acid as the starting material, after ammonolysis, esterification, ester amine solution, split, five-step cyclization reaction Levetiracetam.

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  • 筛选2-代丁酸起始原料氨解,酯化拆分环合五步反应得左乙拉西坦

    Screening for 2 - bromo-butyric acid as the starting material, after ammonolysis, esterification, ester amine solution, split, five-step cyclization reaction Levetiracetam.

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  • 环合废液脱水后,分离回流比为15理论板为40时,回收乙醇甲醇的质量分数小于10%。

    The recovered ethanol with less than 10% methanol can be purified in a dehydration tower and a separation tower with 40 theoretical plates and a reflux ratio of 15.

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  • 以苯甲酰氯为原料,酰化,还原,环合等反应合成左旋西替利嗪盐酸盐,反应收率为8.05%。

    Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation, hydrogenation, cyclization with an overall yield of 8.05%.

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  • 以苯甲酰为原料,酰化,还原,环合等反应合成左旋西替利嗪盐酸盐,反应收率为8。05%。

    Levocetirizine dihydrochloride was prepared from benzoyl chloride by acids lation hydrogenation cyclization with an overall yield of8.05%.

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  • 对比研究不同退火温度对贝组织硬度影响提出了贝氏体球铁辊的退火温度。

    The influences of different annealing temperature on the structure and hardness was compared and investigated. The proper annealing temperature for the bainite nodular iron roller ring was proposed.

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  • 讨论了以草酸二乙酯为原料,经过克莱森缩合、环合氨解反应合成5甲基异唑3甲酰胺工艺改进

    This paper reports the improvement on the synthesis of 5 methylisoxazol 3 formamide by Claisen condensation of diethyl oxalacetate followed by cyclization and ammonolysis.

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  • 方法采用对硝基苯胺为原料,还原保护甲酰化氯化环合、脱保护基六步反应法可进行化学合成。

    Methods Apraclonidine was synthesized from P-Nitraniline by reaction with reduction, adding protection group, formylation, chlorination, cyclization, off-protecting group.

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  • 方法通过付克反应延长水解环合反应得到两个关键中间体,然后通过化反应制得各种酰胺化合物

    METHODS: The title compounds were synthesized by acylation of twelve acyl chlorides and two intermediates prepared by Friedel Crafts reaction, lengthening of carbon chain, hydrolysis and cyclization;

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  • 以对甲苯三氟醋酸乙酯为原料,缩合环合两步反应得到2型环氧抑制剂赛来布,收率为6 7%。

    Celecoxib as a cyclooxygenase-2 inhibitor, was synthesized from p-methylacetophenone and ethyl trifluoroacetate by successively condensation and cyclization in 67% overall yield.

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  • 方法:以氨基乙醛缩甲醇制备的N2 ,2二甲氧基乙基)硫酸盐盐酸催化2 氨基咪唑硫酸盐。

    METHODS:N (2,2 dimethoxylethyl)guanidine sulfate from aminoacetaldehyde dimethyl acetal was treated with concentrated HCl to get 2 aminoimidazole sulfate.

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  • 研究一种直接环合方法,用2-氯-2氯甲基- 4-氰基丁醛三氯反应来制备2-氯-5-氯甲基吡啶。

    A synthetic method of direct cyclization was researched that 2-chloro-2-chloromethyl-4-cyanobutyraldehyde was reacted with phosphorus oxychloride to get 2-chloro-5-chloromethylpyridine.

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  • 研究一种直接环合方法,用2-氯-2氯甲基- 4-氰基丁醛三氯反应来制备2-氯-5-氯甲基吡啶。

    A synthetic method of direct cyclization was researched that 2-chloro-2-chloromethyl-4-cyanobutyraldehyde was reacted with phosphorus oxychloride to get 2-chloro-5-chloromethylpyridine.

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