• 相比目前使用甲醇溶剂纯化收率30%,发现以丙酮乙酸、水的溶剂体系,精制洛韦收率显著提高83.3%,高效液相色谱(HPLC)分析,产品纯度达到99.0%以上。

    Ganciclovir could be purified to more than 99.0%(HPLC) by a combination of acetone, acetic acid and water in 83.3% recovery as compared with 30% one when using water or methanol as solvent.

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  • 确立有机溶剂提取海藻中的生长素乙醚萃取层析法对生长素进行分离纯化方法

    The method of extracting the auxin in seaweeds with organic solvent, separating and purifying the auxin by ether extraction method and column chromatography has been established.

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  • 超声技术可以缩短提取时间溶剂回收有利于下一步鞣质分离纯化更深度的研究

    The ultrasonic extraction can be done in a shorter time, and its solvent is easier to recycle, which is conducive to further separation or purification of tannin or making further study on it.

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  • 目的研究极性有机溶剂辅助阳离子交换色谱串接组合纯化蛋白质可行性

    PurposeTo explore the possibility of combination of anion and cation exchange chromatography by using the polarity organic solvents in eluent.

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  • 研究这类混合溶剂体系可以丰富溶液化学而且盐类分离制备纯化具有重要实际意义

    The study of salt and mixed solvents not only enrich solution chemistry, but also possess important significance to separation preparation and purification of salt.

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  • 反胶萃取技术具有条件温和,萃取效率高成本溶剂重复利用,不引起萃取物变性等优点,用于纯化生物物质前景广阔。

    The use of reversed micelle in extraction of biological molecules has the advantages of mild operational conditions, high extraction efficiency, low cost and solvent recycling.

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  • 通过树皮单宁进行纯化溶剂萃取分级可得到分子量分布范围不同单宁级分。

    Tannin fractions with different molecular weight distributions were obtained by purification of alcohol precipitation and fractionation of solvent extractions of black wattle bark tannins.

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  • 葡萄有机溶剂梯度法酶法提取树脂初步纯化,薄层色谱分离纯化得到花青素单体体。

    The monomer and dimer of proanthocyanidins in grape seeds were obtained by gradient and enzymatic extraction, isolation with macroporous adsorption resin, and purification by TLC.

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  • 反胶萃取技术具有条件温和,萃取效率成本溶剂重复利用,不引起萃取物变性等优点,用于纯化生物物质前景广阔。

    It has a promising profit that extraction of biological molecule by reversed micellar, for the more mild operational condition, higher extraction yield, lower cost and solvent recycling.

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  • 通过溶剂提取次数碱化条件的选择离子交换重结晶方法提取纯化氧化苦参碱。

    Through selecting extracting solvent, extracting times and alkalinizing method, Oxymatrine is extracted and purified by ion-exchanging and re-crystallization.

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  • 再采用空气相色谱法检测所得苹果多酚纯化中正己烷、甲苯、对二甲苯、邻二甲苯、苯乙烯有机溶剂残留均低于检测限。

    There were not n-hexane, benzene, toluene and xylene, o-xylene, styrene and other organic solvent residue in the purification of apple polyphenol by the headspace gas chromatograph.

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  • 本文报道采用分级分离结合有机溶剂沉淀法眼中纯化纯度透明,较其他方法简便,易形成规模。

    This paper deals with the way of purifying highly purity hyaluronic acid from ox eye by fractionation and organic solvent precipitation.

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  • 溶剂萃取法烟碱粗制品纯化,以烟碱和软脂酸反应精制烟碱。

    The unrefined nicotine was purified using solvent extraction and the nicotine was refined by a salification reaction of nicotine and palmitic acid.

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  • 方法考查单体制备纯化溶剂残余聚合方式、引发剂用量、聚合时间、聚合温度因素对聚合的影响

    METHODS Various influencing factors in the preparation of PLA were studied, such as the purity of monomer, the polymerization temperature, and the quantity of the initiator.

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  • 有机溶剂溶剂高压气体沉淀技术结合起来,提出了一种新的蛋白质纯化方法

    A novel method for protein purification was presented, which was the integration of organic antisolvent and compressed gas isoelectric precipitation.

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  • 方法纯净水提取,溶剂萃取大孔吸附树脂硅胶色谱分离等方法分离纯化亚麻根微量成分,通过波谱分析鉴定化合物的结构。

    Method: Isolation and purification of the trace constituents were carried out mainly by solvents extraction and macroporous adsorbing resin and silica gel column chromatography.

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  • 采用溶剂提取色谱法分离纯化大豆粉末磷脂(卵磷脂含量14.05%),得到纯度卵磷脂产品(纯度92.80%)。

    Phosphatidylcholine of high purity(PC, content 92.80%) was prepared from market soybean power phospholipids(PC content 14.05%) by using solvent extraction and column chromatography.

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  • 结果60%丙酮溶剂进行提取,以乙酸乙酯为溶剂进行纯化鞣质纯度达到75%左右,且重复性较

    Results: the purity of tannins can be as high as reach 75% when it's extracted with 60% acetone and purified with ethyl acetate, and the process has good reproducibility.

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  • 萃取分配系数D测定结果表明醋酸乙纯化绿原适用溶剂

    The distribution coefficient D indicated: Ethyl acetate was the most suitable extractant for CGA s purification.

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  • 需要检测合成纯化药物有效成分、赋形剂和医药产品过程使用或产生溶剂

    Therefore, testing should be performed for residual solvents when production or purification processes are known to result in the presence of such solvents.

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  • 高纯甲醇种大量应用于化学微电子工业领域中的重要溶剂脱水工业甲醇纯化精制过程中的一个关键问题

    High purity methanol is one of the very important solvents for chemical industry and microelectronic industry. Dehydration is the key process in the purification of industrial methanol.

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  • 纯化重组蛋白透析冷冻干燥98%甲酸溶剂制备丝蛋白溶液

    The silk fibrous protein solution was prepared by dissolving the recombinant spider silk protein in 98% formic acid after dialyzed and lyophilized.

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  • 乙醇为溶剂重结晶方法纯化胆固醇。

    Besides, the cholesterols were purified by recrystallization.

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  • 表面活性剂作为溶剂广泛应用于LH2分离纯化重构结晶,阐明表面活性剂对LH2的影响非常重要

    Surfactant as solvent widely used in purification, reconstruction and crystallization of LH2. It is very important to reveal the effect of Surfactant on structure and function of LH2.

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  • 表面活性剂作为溶剂广泛应用于LH2分离纯化重构结晶,阐明表面活性剂对LH2的影响非常重要

    Surfactant as solvent widely used in purification, reconstruction and crystallization of LH2. It is very important to reveal the effect of Surfactant on structure and function of LH2.

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