F2水液丙酮沉淀纯化后,上c 18反相柱反复纯化。
F2 water purification liquid acetone precipitation, the RP-C18 column repeated purification.
报道反相离子对及离子抑制色谱分析几种不同类型药物的分离条件,同时对这些药物在C18反相柱上的色谱行为进行了研究。
The separation conditions of several drugs by reversed-phase ion pair and ion suppression HPLC were described, respectively. Their chromatographic behaviour on the C18 columns was studied.
洗脱物经预柱脱盐和浓缩后进入毛细管反相柱进行反相分离,分离后的肽段直接进入质谱仪离子源进行一级和二级质谱的分析。
Following desalinisation the eluted peptides were further purified by reversed-phase capillary column(150 mm 75 m) and online analysed by the coupled tandem mass spectrometry.
采用高效液相色谱法,使用反相色谱柱和二极管阵列检测器测定吡·哒可湿性粉剂中吡虫啉和哒螨灵的含量。
Using reversed-phase chromatographic column and diode array detector, content of imidacloprid and pyridaben in their water soluble powder was measured with high effective liquid chromatography.
本方法采用反相色谱柱分离,三元混合流动相进行洗脱,紫外可变波长检测器进行检测,以外标法定量。
The examining method is that using reversed-phase chromatograph module to separate, three mixture mobile phase to wash drop, UV flexible wavelength to detect, external standard method to get contents.
建立了反相高效液相色谱法测定辐花肋柱花中苦龙苷的含量。
In this article, RP-HPLC was applied to determine the content of amarogerth in Lomatogonium rotatum.
方法利用正相、反相硅胶柱和大孔树脂柱色谱分离,并通过波谱技术进行结构鉴定。
Methods The compounds were isolated by silica gel, ODS, and macroporous resin column chromatography and their structures were determined by means of spectral analysis.
方法采用硅胶和反相硅胶RP- 18柱色谱分离,运用有机波谱分析确定化合物结构。
Methods Three compounds were isolated by a combination of RP-18and silica gel column chromatographies, and their structures were identified by spectral methods.
以异丙醇为柱前衍生试剂,建立了反相高效液相色谱法间接测定2-乙酰氧基异丁酰溴的新方法。
A rapid reverse high performance liquid chromatography method based on the iso - propyl alcohol as an agent of pre-derivatization is developed for the determination of 2-acetoxyisobutyryl bromide.
方法采用柱色谱法分离,反相高效液相色谱法与细胞膜色谱法联用,并结合离体药理实验确定太白花中的有效成分。
METHOD S The effective component was determined by cell membrane chromatography and reversed phase high performance liquid chromatography. The pharmacological actions in vitro were testified.
建立了柱前衍生反相高效液相色谱法测定奶粉及其他乳制品中L-羟脯氨酸的方法。
The method of determining hydroxyproline(Hyp) in milk powder and other dairy products was developed by pre-column derivation RP-HPLC.
用这种方法合成的万古霉素苯异氰酸酯手性色谱固定相填料装柱后,可以在正相、反相及极性有机相色谱条件下使用。
The chiral chromatographic fixed phase stuffing of vancomycin phenylisocyanate after assembled to column may be used in forward phase, reverse phase and polar organic phase chromatographic condition.
其中液相色谱反相填料,正相填料,生物工程用大孔硅胶,样品预处理净化富集柱以及微孔滤膜、滤器均已达到国际先进水平。
The liquid chromatography Silica and bonded silica gel, macro-porous silica gel for bio-engineering, SPE column and microprobe filters has reached advanced world standard.
其中液相色谱反相填料,正相填料,生物工程用大孔硅胶,样品预处理净化富集柱以及微孔滤膜、滤器均已达到国际先进水平。
The liquid chromatography Silica and bonded silica gel, macro-porous silica gel for bio-engineering, SPE column and microprobe filters has reached advanced world standard.
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