采用正交设计法,选择L9(34)表,研究N-乙酰-L-亮氨酸的合成,提高反应得率。
Using orthogonal design method, adopting L9 34 table, to research the synthesis of N-acetyl-L-leucine, for improving the productive rate.
文中对酰胺羰基化反应条件进行了优化,分离得到消旋N-乙酰基亮氨酸产率为66.4%。
The amidocarbonylation reaction conditions were optimized and 66.4% isolated yield of racemic N-acetylleucine were obtained.
文中对酰胺羰基化反应条件进行了优化,分离得到消旋N-乙酰基亮氨酸产率为66.4%。
The amidocarbonylation reaction conditions were optimized and 66.4% isolated yield of racemic N-acetylleucine were obtained.
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