实验以盐酸三乙胺-三氯化铝离子液体(IL)为催化剂,催化水杨酰胺(SA)与乙酰氯进行傅克酰基化反应合成5乙酰水杨酰胺。
Friedel-Crafts acetylation of salicylamide(SA) with acetyl chloride to 5-acetylsalicylamide using triethylammonium chloroaluminate ionic liquid(IL) as both catalyst and solvent was investigated.
通过对利用本发明的方法制备的6-酰基蔗糖氯化和去乙酰化可以制备氯化蔗糖,强力甜味剂三氯半乳蔗糖。
Chlorinated sucrose, the high intensity sweetener trichlorogalactosucrose can be prepared by chlorination and deacylation of 6-acyl sucrose prepared by the process of this invention.
以蔗糖为起始原料,经羟基选择性保护、氯化、脱乙酰基等3步化学反应合成三氯蔗糖;
Sugar was as the start material by the reaction of the selective protections at 6-hydroxy, chlorination, deacetyl in three steps obtained the target compound(trichlorosucrose);
以蔗糖为起始原料,经羟基选择性保护、氯化、脱乙酰基等3步化学反应合成三氯蔗糖;
Sugar was as the start material by the reaction of the selective protections at 6-hydroxy, chlorination, deacetyl in three steps obtained the target compound(trichlorosucrose);
应用推荐