• 制备出一种柱效高、成本低的复合型色谱柱。

    A new high efficient and low cost packed column with mixed stationary liquids is prepared.

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  • 考察了这种固定相的柱效、热稳定性、极性及选择性等色谱特性。

    The chromatographic characteristics, including column efficiency, thermal stability, polarity and selectivity were studied.

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  • 由结果推测,温度升高,将显著提高离子交换法吸金过程的色谱柱效。

    It can be predicted from the results that the column effect of adsorption of gold by ion exchanger will be remarkably improved by increasing temperature.

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  • 与卫生部药品标准方法相比,柱效提高、拖尾现象减小,杂质分离更加有效。

    Compared with the current method, this method was better in the column efficiency, less tailing and effective separation of impurities.

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  • 对未完全损伤的柱子,以老化色谱柱提高柱效,严重损伤、老化者,应更换新柱;

    Badly damaged or aged chromatogram column should be substituted by new ones, if not fully damaged, it could be improved by aged chromatogram column.

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  • 用自由区带毛细管电泳分离时,分离缓冲液中加入40%乙腈可显著提高柱效和灵敏度。

    Adding 40%acetonitrile to the borate running buffer significantly improved the separation efficiency and the fluorescence detection sensitivity.

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  • 适当的高柱温既保留了部分包结作用,同时存在端口协同作用,能兼顾高选择性和高柱效。

    Therefore, properly high column temperature can balance between high column efficiency and high selectivity via partial inclusion complexation and portal synergetic interactions.

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  • 该柱具有柱效高、惰性好热稳定性好的色谱特性;用于二甲苯异构体的分析具有很好的选择性。

    It has chromatographic performance of high column efficiency, good inertia and thermal stability, very high selectivity on analyzing dimethylbenzene isomer.

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  • 结果表明,该法能有效检测头孢克肟的中间体,具有柱效高、经济等优点,可用于头孢克肟反应过程的监测。

    The results show that the method can detect the content of cefixime intermediates effectively and economically. This HPLC method can be used to monitor the cefixime reaction process.

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  • 结果表明,溶质的径向扩散不仅对柱效、峰展宽、峰形特征等有影响,而且对溶质的保留时间也有一定的影响。

    The results show the radial diffusion affects not only the column efficiency, the peak spreading and the peak symmetry, but also the retention time.

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  • 用其涂渍的弹性石英管柱柱效较高,使用温度范围较宽,热稳定性和选择性较好。研究了固定液对样品的分离机理。

    Its chromatographic characteristics including column efficiency, operating temperature range, thermal stability, polarity and selectivity were studied, and its separation mechanism was discussed.

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  • 这一方法转化软件可以立即对温度、流速进行计算以适应各种要求,包括保留时间锁定,最高理论柱效和缩短分析时间。

    The method translation software will instantly calculate temperature and flow conditions to meet various requirements including retention time locking, best theoretical efficiency, and decreased time.

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  • 本文综述了高温条件下,温度对柱效、保留值、选择性、溶剂洗脱特征及色谱柱稳定性的影响,介绍了高温色谱的应用进展。

    The effects of temperature on column performance, retention, selectivity, and column stability are reviewed and applications of HTLC are introduced in this paper.

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  • 考察了温度、流速和流动相组成对酚类样品的保留、分辨、柱效和系统压力的影响,探讨了酚类样品在聚合物柱上的热力学行为。

    The effects of temperature, flow rate and composition of mobile phase on retention, resolution, column efficiency and the pressure of the system were examined.

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  • 考察了温度、流速和流动相组成对酚类样品的保留、分辨、柱效和系统压力的影响,探讨了酚类样品在聚合物柱上的热力学行为。

    The effects of temperature, flow rate and composition of mobile phase on retention, resolution, column efficiency and the pressure of the system were examined.

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