该文研究了微波辐射和常规加热下卤素交换氟化合成对氟硝基苯的方法,提出了共沸干燥和微波干燥制备无水KF的方法。
The halogen exchange method to prepare p fluoronitrobenzene under microwave irradiation and conventional heat was studied. Drying KF by azeotropy and microwave irradiation was proposed.
提出了一种以2,3-二氯硝基苯为原料,经氟化、高温氯化、硝化、再氟化反应合成2,3,4-三氟硝基苯的新工艺路线。
A method is given for synthesis of 2,3,4 trifluoronitrobenzene from 2,3 dichloronitrobenzene by fluorination, chlorination, nitration, etc.
提出了一种以2,3-二氯硝基苯为原料,经氟化、高温氯化、硝化、再氟化反应合成2,3,4-三氟硝基苯的新工艺路线。
A method is given for synthesis of 2,3,4 trifluoronitrobenzene from 2,3 dichloronitrobenzene by fluorination, chlorination, nitration, etc.
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