• NMR spectra are often calibrated against the known solvent residual proton peak instead of added tetramethylsilane.

    核磁共振谱通常是根据已知的溶剂残留质子峰进行校正,而不是添加四甲基硅烷。

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  • Their ir and NMR spectra were measured.

    测定了它们的红外光谱和核磁共振波谱。

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  • The structure was confirmed by FTIR and NMR spectra.

    并通过质谱、红外谱图和核磁共振谱确认了其结构。

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  • The new compounds were also characterized by NMR spectra and HRMS.

    这些新化合物同样得到了核磁波谱和高分辨质谱的表征。

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  • The products were characterized by elemental analysis, IR and 1h NMR spectra.

    通过元素分析、红外光谱和1h NMR对产物进行了表征。

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  • The character of NMR spectra was an important proof to judge the reactive place.

    NMR图谱的特征是判断葛根素反应位点的一个重要标志。

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  • The 13C-NMR and 1H-NMR spectra were reported for the macrocyclic polyaryl-ester oligomer.

    本文报道了环状聚芳酯低聚物的核磁共振碳谱及氢谱。

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  • The occurrence of SBR cyclization was confirmed by the primary analysis of ir and 1 H-NMR spectra.

    通过对红外光谱、1H - nmr谱的初步解析,证实了环化反应的发生。

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  • Based on classical and quantum theories, dynamic NMR spectra are simulated by means of DJS-130 computor.

    本文在经典和量子理论的基础上,用国产DJS - 130机对核磁共振中的动态谱进行模拟。

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  • The product has been characterized in detail by elemental analysis, infrared, UV, NMR spectra, DSC and TG etc.

    其产品的特性用元素分析,红外和紫外光谱,NMR,DSC,TG等进行了详细地表征。

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  • These compounds have not been reported before, and the structures were identified by MS, IR and 1h-nmr spectra.

    合成的化合物均未见文献报道,其结构通过了MS、IR以及1 H - NMR谱确证。

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  • This paper deals with the structural formula of polyethylene glycol quaternary ammonium by the 13C-NMR and 1H-NMR spectra.

    本文着重从核磁共振光谱的角度(包括氢核磁共振谱和碳核磁共振谱)来研究多甘醇单甲醚季铵盐的结构。

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  • The title compound was synthesized with phenanthrenequinone as starting material and was characterized by IR and 1H NMR spectra.

    以菲醌为原料合成了标题化合物,通过IR和1H NM R对其结构进行了表征。

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  • Some typical studies on the grafting and crosslinking of gelatin by NMR spectra were Presented. The analytical method was introduced.

    通过NMR谱图对明胶的几个典型接技、交联反应进行研究,介绍了反应的微观情节及NMR谱图用于该研究的大致方法。

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  • NMR spectra of 12 titled compounds are determined. The chemical shifts of 1h and 13c and the data of quantitative analysis are reported.

    测定了12个标题化合物的核磁共振谱,报道了它们的1h和13C化学位移以及定量分析数据。

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  • The product was characterized by elemental analysis, melting point, IR and NMR spectra and was found to be in accordance with the expected compound.

    它被广泛用作聚酚亚胺材料的单体,国内尚无市售,经元素分析,熔点,IR,NMR表征,表明结果与预期产物相符。合成步骤简单,原料易得。

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  • METHODS Recording the 1D and 2D NMR spectra of lomerizine dihydrochloride while changing the experimental temperature and adding D 2O into the solution.

    方法测定其在改变温度和加入重水条件下的各种1D和2 D核磁共振谱。

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  • Sodium acrylate-vinyl acetate random copolymers with different composition were synthesized and characterized, and the peculiar NMR spectra were presented.

    合成了不同组成的丙烯酸钠-醋酸乙烯酯无规共聚物,并对其作了表征,给出了奇特的NMR谱。

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  • Method: Separating the constituents by means of chromatography and identifying their structures on the basis of NMR spectra and TLC with authentic samples.

    方法:硅胶柱色谱等方法分离,薄层色谱和波谱分析鉴定结构。

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  • Molybdophosphoric acid used as the catalyst, two alkyl glycolates were prepared. The glycolates were characterized by the boiling points and proton NMR spectra.

    以钼磷酸为催化剂合成了两种羟基乙酸酯,并经沸点和核磁共振氢谱确定了它们的组成和结构。

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  • The IR and NMR spectra of the polymers indicated that the polymer structure contained ester and ketone units in the backbone, and a cyclic acetals as side chain.

    通过对该合聚物的IR和NMR谱图分析,得知该聚合物含有酯基和酮基的结构单元,以及环缩醛的侧链。

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  • Objective By analyzing the NMR spectra of analogs of Baogongteng a, tropane alkaloids, the effects of structural variations on chemical shifts of resonance signals were investigated.

    目的通过对包甲素类似物nmr谱的分析,考察其结构差别对共振信号化学位移的影响。

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  • Three photochromic N, N'-1,4-tetramethylene bisspiropyran and bisspirooxazine compounds were synthesized. They have been identified by IR spectra, 1H -NMR spectra and elemental analysis;

    合成三种N,N'-1,4-亚丁基双螺吡喃和双螺恶嗪光致变色化合物,通过红外光谱、核磁共振氢谱及元素分析确证其结构。

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  • A novel metal chromium containing organic monomer, N vinylcarbazole chromium tricarbonyl has been synthesized and the structure has been confirmed by elemental analysis, IR and 1H NMR spectra.

    合成一种新的金属铬有机单体N -乙烯基咔唑三羰基铬,经元素分析、IR和1H NMR确证和表征。

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  • The results obtained from the determination of sequence structure of copolyamide of HDA-PPD-TPC showed that the method can be used for copolycondensation polymers with overlapping peak NMR spectra.

    该法在HDA-PPD-TPC三元共聚酰胺体系序列结构研究中应用,证明具有较好的适应性和准确性。

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  • The techniques have advantages over conventional single quantum NMR method in obtaining simple analyzable spectra which make study of molecular structure and conformation possible.

    多量子NMR能得到比寻常NMR方法简单的解析谱,从而增进了研究分子结构和构型的可能性。

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  • Compared with that of lignin sulfonic acid, the spectra of UV, 1h NMR and IR were changed apparently.

    其氧化产物的紫外吸收光谱、1h核磁共振谱和红外光谱有明显改变。

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  • The complexes have been isolated chromatographically and characterized by elemental analysis, electron absorption spectra, infrared spectra and1H NMR spectroscopy.

    诸配合物通过层析色谱柱分离,并用元素分析、电子光谱、红外和1h核磁共振所表征。

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  • The pyrazoles ramification containing dithioether is synthesized by one-step method and characterized by H-NMR, IR and UV-Vis spectra.

    并采用氢核磁共振,红外光谱和紫外吸收光谱等手段进行了表征。

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  • The pyrazoles ramification containing dithioether is synthesized by one-step method and characterized by H-NMR, IR and UV-Vis spectra.

    并采用氢核磁共振,红外光谱和紫外吸收光谱等手段进行了表征。

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