The reactions were carried out in an isocratic reactor and an oil bath fixed bed reactor, which are designed by us.
反应是在实验室自行设计的无梯度反应器和油浴固定床反应器中进行。
Diastereomers of cinchonine and cinchonidine were fully separated both under isocratic and gradient elutions on the chiral monolithic column.
在等度及梯度洗脱条件下，非对映异构体辛可宁与辛可尼丁被完全分离。
Then, I use another 10-min gradient to reequilibrate from the final conditions back to the initial conditions, followed by 8 min of isocratic hold.
然后，我用另外10分钟的梯度把最终的条件重新平衡到初始的条件，接着保持8分钟等度洗脱。
This isocratic system consists of a high pressure solvent delivery pump, an UV/VIS detector, a manual injection valve, and a solvent tray, a column and a Chromatography Workstation.
整套系统由高压输液泵、检测器、进样阀、溶剂托盘、色谱柱、工作站软件等组成；
This isocratic system consists of a high pressure solvent delivery pump, an UV/VIS detector, a manual injection valve, and a solvent tray, a column and a Chromatography Workstation.
整套系统由高压输液泵、检测器、进样阀、溶剂托盘、色谱柱、工作站软件等组成；
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