• A possible mechanism for the cyclization reaction was suggested.

    提出了可能的环化反应机理。

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  • The major process to study DNA instinctive flexibility is DNA cyclization assay.

    DNA分子的环化是研究其本身柔韧性的主要方法。

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  • The appropriate reaction conditions of cyclization reaction: NaOEt was 1.4 mole eq.

    合环反应的条件为:乙醇钠的用量为1.4摩尔当量;

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  • The mechanism was discussed in the proton acid catalytic reaction of furan phenol cyclization.

    探讨了呋喃酚环合反应质子酸催化机理。

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  • The phenomonon was explained in view of the mechanism of chemical cyclization of poly(amic acid).

    从聚酰胺酸化学环化反应机理出发对这一结果给予了解释。

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  • The mechanism of cyclization of DAT and the principle of the anion extraction were also discussed.

    同时,探讨了DAT的成环反应历程,阐述了阴离子高效萃取的原理。

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  • The theory involving the cyclization effect was in excellent agreement with the experimental data.

    经过适当内环化校正的理论与实验数据很好地符合。

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  • The occurrence of SBR cyclization was confirmed by the primary analysis of ir and 1 H-NMR spectra.

    通过对红外光谱、1H - nmr谱的初步解析,证实了环化反应的发生。

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  • The method adopts the amino resin to synthesize carbetocin by the solid phase cyclization technology.

    本发明采用氨基树脂,固相环合技术,合成卡贝缩宫素。

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  • The conditions of reaction of cyclization were moderate, the purity and yield of the product was higher.

    环合反应的条件缓和,产品收率和纯度高,在四氢咔唑类化合物的化学制备中具有重要参考价值。

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  • According to the experimental results, it was assumed that the cyclization was taken by nucleophilic attack.

    根据实验结果,我们推测反应的关键步骤为亲核进攻。

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  • METHODS Bretazenil was synthesized from 3-bromoaniline by cyclization, oxidation and ring-enlargement reaction, etc.

    方法以3-溴苯胺为起始原料,经过成环、氧化、扩环等反应得到目标产物。

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  • Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation, hydrogenation, cyclization with an overall yield of 8.05%.

    以苯甲酰氯为原料,经酰化,还原,环合等反应合成左旋西替利嗪盐酸盐,反应总收率为8.05%。

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  • From 2, 6-dichloropyridine as starting material, we can get the target molecule through nitration, substitution, reduction, cyclization, oxidation etc.

    以2,6 -二氯吡啶为原料,通过硝化,取代,还原,环化,氧化等几步反应可得到目标化合物。

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  • In another direction, the radical cyclization of thioimide with acylsilane produced simple cyclization product in low yield without expected enol silyl ether compound.

    对于硫醯亚胺与矽基酮的自由基反应,则是得到低产率的简单环化产物,而不是预期的烯醇矽醚化合物。

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  • This paper reports the improvement on the synthesis of 5 methylisoxazol 3 formamide by Claisen condensation of diethyl oxalacetate followed by cyclization and ammonolysis.

    讨论了以草酸二乙酯为原料,经过克莱森缩合、环合、氨解反应合成5甲基异唑3甲酰胺工艺的改进。

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  • Methods Apraclonidine was synthesized from P-Nitraniline by reaction with reduction, adding protection group, formylation, chlorination, cyclization, off-protecting group.

    方法采用对硝基苯胺为原料,经还原、加保护基、甲酰化、氯化、环合、脱保护基六步反应法可进行化学合成。

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  • Bromacil was synthesized using 2-bromobutane and urea as the starting materials in three steps including condensation, cyclization and bromination with total yield of 61%.

    以2 -溴丁烷和尿素作为起始原料,经缩合、环化、溴代三步反应得到除草定,总收率为61%。

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  • By adjusting the reaction temperature or using different cyclization methods, condensation is carried out, and indanone dimmer and indanone trimer can be obtained respectively.

    然后进行缩合,通过调节反应温度或者使用不同的环化方法,可分别得到茚酮的二聚物及三聚物。

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  • The invention relates to a cyclopeptide analog and a cyclization method thereof, which aims at providing an integrin ligand cyclopeptide analog and a cyclization method thereof.

    本发明涉及环肽类似物及其环化方法,旨在提供一种整合素配体环肽类似物及其环化方法。

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  • The cracking and skeletal isomerization became more strong with the rise of reaction temperature, while oligomerization, cyclization and hydrogen transfer reaction became weaker.

    随着反应温度的提高,裂化反应和骨架异构化反应增强,但齐聚反应、氢转移反应和环化反应减弱。

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  • Celecoxib as a cyclooxygenase-2 inhibitor, was synthesized from p-methylacetophenone and ethyl trifluoroacetate by successively condensation and cyclization in 67% overall yield.

    以对甲苯乙酮和三氟醋酸乙酯为原料,经缩合、环合两步反应得到2型环氧酶抑制剂赛来昔布,总收率为6 7%。

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  • The mechanism of in-situ cyclization during the foaming and heat treatment was studied using differential scanning calorimeter (DSC) and Fourier transform infrared spectrometer (FTIR).

    探讨了相应共聚物在发泡和热处理过程中发生的“原位成环”反应及机理,并利用差示扫描量热分析(DSC)和红外光谱(FTIR)进行了验证。

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  • Methods:Starting from 5-cyanophthalide, escitalopram oxalate was prepared via several steps including nucleophilic addition, hydrolysis, chemical separation, cyclization and salt formation.

    方法:以5-氰基苯酞为起始原料,经亲核加成、水解、化学拆分、环化和成盐等反应制得抗抑郁药草酸依地普仑。

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  • Methods:Starting from 5-cyanophthalide, escitalopram oxalate was prepared via several steps including nucleophilic addition, hydrolysis, chemical separation, cyclization and salt formation.

    方法:以5-氰基苯酞为起始原料,经亲核加成、水解、化学拆分、环化和成盐等反应制得抗抑郁药草酸依地普仑。

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