研究了2-羟基-5-磺酸苯基重氮氨基偶氮苯(HSDAA)与镉的反应,建立了直接测定铝合金中镉的光度分析方法。
The reaction of 2-hydroxy-5-sulfophenyl-diazoaminoazobenzene (HSDAA) with cadmium was studied to establish the direct photometric determination of cadmium in aluminum alloy.
本文以对氨基苯乙酮和二茂铁为底物,在相转移催化剂存在的条件下发生重氮芳基化反应。
In this paper, we investigated the arylation reaction ofp-amino acetylbenzene with ferrocene catalyzed by phase transfer catalyst.
采用自行设计制造的重氮甲烷发生装置,有效控制了二甲基亚硝基苯磺酰胺的反应用量,减少了有害气体的排放。
By adopting the self-designed diazomethane generating device, the dosage of reaction reagent of diazald was effectively controlled and the harmful gas release was reduced.
重氮甲烷与酸性除草剂发生衍生反应,生成易于气相色谱-质谱测定的酯类化合物,反应条件温和,副产物少。
Under mild reaction condition, the derivative reaction of diazomethane with acid herbicides occurred and produced ester compounds with little by-products, which could be easily detected by GC-MS.
二氢-2-甲基-4-苯基-1,5-苯并硫氮杂卓与重氮乙酸乙酯反应,得到非预期的分子内重排的开环产物。
From the reaction of 2,3 dihydro 2 methyl 4 phenyl 1,5 benzothiazepines with diazozcetic ester an unexpected ring open product of the intramolecular rearrangement was obtained.
文章介绍了利用实验室常见物品制作简易重氮甲烷发生和反应装置的步骤。
The paper described the method of making diazomethane and its corresponding apparatus by using common items in the lab. All the required materials were low cost and easy to obtain.
文章介绍了利用实验室常见物品制作简易重氮甲烷发生和反应装置的步骤。
The paper described the method of making diazomethane and its corresponding apparatus by using common items in the lab. All the required materials were low cost and easy to obtain.
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