间苯氧基苯乙酮可由酚钾与间溴苯乙酮在醋酸铜催化下以高产率合成。
Phenoxyacetophenone could be prepared from potassium phenolate and m bromoacetophenone via Ullmann reaction catalyzed by copper acetate in high yields.
结果表明乙二醇与醋酸钾的混合物是分离甲乙酮水二元恒沸物的理想萃取剂。
The separation of azeotrope of methyl ethyl ketone water has been investigated by extractive distillation using the mixture of ethylene glycol and potassium acetate as an extractant.
建立了高效液相色谱法测定妊娠双烯醇酮醋酸酯合成工艺中裂解和氧化、水解两部分产品的分析方法。
A method of HPLC has been established for quantitative determination of concentrations of acetolysis and hydrolysis solutions in the synthesis technology of 16 _ dehydropregnenolone acetate.
在醋酸、聚乙二醇存在下,铬酸酐和苊在温和的条件下反应,苊可以完全转化为苊酮。
In the presence of acetic acid and polyethylene glycol, chromic anhydride and acenaphthene react under mild condition and acenaphthene can completely convert into acenaphthenone.
酮的对甲苯磺酰腙在含水的乙腈中与聚苯乙烯二醋酸磺苯在温和条件下反应得到高产率的酮。
Reaction of tosylhydrazones of ketones with CPSID in wet acetonitrile affords the corresponding parent ketones in excellent yields under mild conditions.
方法青蒿可溶性糖含量测定使用蒽酮醋酸乙酯法,青蒿游离氨基酸含量测定用茚三酮比色法。
Methods Saccharide content was determined by anthracene ethyl ketone method; amino acid content was estimated by indene tri-ketone colorimetric method.
以对甲苯乙酮和三氟醋酸乙酯为原料,经缩合、环合两步反应得到2型环氧酶抑制剂赛来昔布,总收率为6 7%。
Celecoxib as a cyclooxygenase-2 inhibitor, was synthesized from p-methylacetophenone and ethyl trifluoroacetate by successively condensation and cyclization in 67% overall yield.
以对甲苯乙酮和三氟醋酸乙酯为原料,经缩合、环合两步反应得到2型环氧酶抑制剂赛来昔布,总收率为6 7%。
Celecoxib as a cyclooxygenase-2 inhibitor, was synthesized from p-methylacetophenone and ethyl trifluoroacetate by successively condensation and cyclization in 67% overall yield.
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