实验结果表明,反应温度和溴代正丁烷的用量是相转移催化合成噻酮工艺的主要影响因素。
The experimental results indicated that the reaction temperature and the dosage of 1-butyl bromide were the main factors while the reaction time and the dosage of TBAB were the minor factors.
本实验采用氢溴酸法,用浓硫酸作催化剂,以正辛醇、工业废氢溴酸(48%)及浓硫酸为原料,合成1 -溴代正辛烷。
N-octyl bromide was synthesized by hydrobromic method in which took n-octanol and industrial waste hydrobromic acid (48%) as materials, concentrated sulfuric acid as a catalyst.
本实验采用氢溴酸法,用浓硫酸作催化剂,以正辛醇、工业废氢溴酸(48%)及浓硫酸为原料,合成1 -溴代正辛烷。
N-octyl bromide was synthesized by hydrobromic method in which took n-octanol and industrial waste hydrobromic acid (48%) as materials, concentrated sulfuric acid as a catalyst.
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