以2 -溴丁烷和尿素作为起始原料,经缩合、环化、溴代三步反应得到除草定,总收率为61%。
Bromacil was synthesized using 2-bromobutane and urea as the starting materials in three steps including condensation, cyclization and bromination with total yield of 61%.
制备1 -溴丁烷是有机化学实验中的一个具有代表性的卤代烃合成实验。
Preparation of 1-bromo-butane experiments in organic chemistry are a representative experiment halohydrocarbon synthesis.
实验结果表明,反应温度和溴代正丁烷的用量是相转移催化合成噻酮工艺的主要影响因素。
The experimental results indicated that the reaction temperature and the dosage of 1-butyl bromide were the main factors while the reaction time and the dosage of TBAB were the minor factors.
实验结果表明,反应温度和溴代正丁烷的用量是相转移催化合成噻酮工艺的主要影响因素。
The experimental results indicated that the reaction temperature and the dosage of 1-butyl bromide were the main factors while the reaction time and the dosage of TBAB were the minor factors.
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