本文研究了3-氰基吡啶微生物转化产物的反相高效液相色谱(RP-HPLC)分析方法。
The conditions for the analysis of transformed products of 3-cyanopyridine via microorganism by RP-HPLC with flow rate gradient of mobile phase have been studied.
以4甲基吡啶为原料,在固定床反应器中通过含氧化钒的催化剂发生气固相接触氨氧化反应制备雷米封中间体4氰基吡啶,4甲基吡啶的转化率为99%,4氰基吡啶的选择性为88%,收率为87。
4-cyanopyridine, intermediate of rimifon, was synthesized from 4-picoline using vanadium oxide as a catalyst in a fixed-bed reactor, reached 99% conversion of 4-picoline, 88% selectivity and 87.
研究了用烷基吡啶基聚苯乙烯树脂(BPR)从氰化液中吸附各种金属氰离子。
The adsorption of many metal cyanides from alkali cyanide solutions using BPR resin was investigated.
研究了一种直接环合的方法,用2-氯-2氯甲基- 4-氰基丁醛与三氯氧磷反应来制备2-氯-5-氯甲基吡啶。
A synthetic method of direct cyclization was researched that 2-chloro-2-chloromethyl-4-cyanobutyraldehyde was reacted with phosphorus oxychloride to get 2-chloro-5-chloromethylpyridine.
本文用2-氯-5-氯甲基吡啶经氨基化,和N-氰基乙亚胺酸乙酯反应,最后甲基化得到吡虫清。
In this thesis, 2-chloro-5-chloromethyl pyridine is ammoniated, which followed by the reaction with N-cyano ethyl ethylimidoate, finally is methylated to gain the objective product.
本文用2-氯-5-氯甲基吡啶经氨基化,和N-氰基乙亚胺酸乙酯反应,最后甲基化得到吡虫清。
In this thesis, 2-chloro-5-chloromethyl pyridine is ammoniated, which followed by the reaction with N-cyano ethyl ethylimidoate, finally is methylated to gain the objective product.
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