介绍了氯代环己烷的合成工艺及其应用。
The synthetic process and application of cyclohexyl chloride are introduced.
有机氯类用乙酸乙酯—环己烷和凝胶净化柱提取净化，石英毛细管气相色谱(配ecd检测器)检测。
Organic chlorine using ethyl acetate - cyclohexane and gel purification column extraction purification, quartz capillary gas chromatography (ECD allocation) detection.
溶剂采用环己烷、1,2 -二氯乙烷、吡啶中一种或多种混合使用。
The solvent is used by adopting one of or mixture of more than one of cyclohexane, 1, 2-dichloroethane and pyridine.
以二氧杂环己烷为溶剂，通过聚乙二醇2 70与对甲基苯磺酰氯反应合成了1 8冠6，产率64 .4 %。
Also, in dioxane solution, 18Crown6 was prepared in 64.4% yields by reaction of polyethylene glycol 270 and ptoluenesulfonyl chloride.
以二氧杂环己烷为溶剂，通过聚乙二醇2 70与对甲基苯磺酰氯反应合成了1 8冠6，产率64 .4 %。
Also, in dioxane solution, 18Crown6 was prepared in 64.4% yields by reaction of polyethylene glycol 270 and ptoluenesulfonyl chloride.
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