实验结果表明,电解的电流效率和邻甲基苯甲醛、间甲基苯甲醛的合成产率在超声的参与下有10 %左右的提高。
The experimental results indicated that the current efficiency of electrolysis and the yields of o-, m-, p-methylbenzaldehydes were promoted about 10% under ultrasound irradiation.
研究了强碱氢氧化钾加入量和溶剂等对反应的影响,发现随着碱浓度的增加,邻硝基甲苯的转化率增加,邻硝基苯甲醛的收率先增后降。
The effect of strong base, KOH, was studied and it was found that the conversion of o-nitrotoluene increased if the amount of KOH increased.
羟基处于醛基邻位和对位的苯甲醛与几种苯乙酮衍生物的缩合,多数没有得到预期的产物,或收率极低;苯乙酮环上的羟基对缩合反应影响很大,羟基越多,缩合越困难。
The groups in ring of benzaldehydes, no matter they are electron withdrowing or electron donating except of hydroxy, do not seem to have much effect on the yield.
研究了在稀碱催化下邻羟基苯乙酮和苯甲醛在乙醇溶液中的羟醛缩合反应,溶剂可以循环使用,适合工业化生产。
During the condensation reaction, the feedstock remaining after reaction can be recycled, and this synthesis route was suitable for the commercial production.
由邻甲苯胺和甲醛水溶液反应合成得到了高纯度的3,3 -二甲基-4,4 -二氨基二苯甲烷(MDT),并对其性能进行了表征。
The polyimide monomer of 3,3 -dimethyl-4,4 -diaminodiphenylmethane(MDT)was synthesized through the reaction between O-methyl aniline and aqueous formaldehyde solution.
由邻甲苯胺和甲醛水溶液反应合成得到了高纯度的3,3 -二甲基-4,4 -二氨基二苯甲烷(MDT),并对其性能进行了表征。
The polyimide monomer of 3,3 -dimethyl-4,4 -diaminodiphenylmethane(MDT)was synthesized through the reaction between O-methyl aniline and aqueous formaldehyde solution.
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