• 综述近年来国外关于六甲基二硅烷合成工艺还原合法、格氏试剂法、电解还原);就其未来的研究方向提出了建议。

    The synthesis methods of hexamethyldisilane, such as reductive coupling reaction, Grignard reagent alkylation, electrochemical reduction et al, were recounted in details.

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  • 这个过程包括氧化钛反应润滑脂分钟

    The process involves taking titanium dioxide and treating it with silica, silicone grease or silicic acid for a few minutes.

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  • 方法简单反应周期得到纯度达98%甲基环己基甲氧基硅烷产品

    The method simple, the reaction period short and the productive rate high. The purity of the product can reach 98%.

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  • 结果表明,使用环己基- 甲基-硅烷聚合物等规可调性好;

    With cyclohexyl methyl dimethoxy silane(CHMMS) as external donor, isotacticity of polymer turned to be more adjustable.

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  • 采用正交实验设计研究反应温度升温速率乙烯基苯质量分数裂解温度保温时间五个因素聚碳率的影响。

    Based on orthogonal design, the effects of reaction temperature, heating speed, weight percent of DVB, pyrolysis temperature and heat retaining time on the yield of PCS were discussed.

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  • 硅烷偶联KH550为桥梁,利用酰胺反应改性HBPE(记做MHBPE)氧化钛表面

    By use of silane coupling agent KH550 the modified HBPE (MHBPE) was grafted onto the surface of ultrafine titanium dioxide by amidation reaction.

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  • 考察了硅烷偶联KH-550聚丙烯PP)/溴新戊磷酸PEA复合体系中的增容作用。

    The effect of silane coupling agent KH-550 as a compatibilizer in polypropylene (PP)/phosphate ester dibromoneopentyl glycol acid (PEA) composites was studied.

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  • 研究苯基硅烷双酚-A等克分子条件下缩聚反应动力学

    The kinetics of the polycondensation between diphenyl-dichlorosilane and bisphenol-A in equal mole ratio has been studied.

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  • 新增投入运行,经甲基硅烷纯度、水裂解工序操作性产品质量等指标验证达到预期的效果

    When new tower put into use, verifying the purity of dimethyldichlorosilane, operability of hydrolyzed and cracked process and product quality, it got the desired results.

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  • 探讨氧基硅烷封端率及端羟基聚丁含量单组分密封力学性能硬度时间影响

    The effects of different silane end-capped ratios and HTPB content on mechanical properties, hardness and surface dry time of the sealant were discussed.

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  • 研究载液相催化剂制备及其3-氯丙烯与甲基加成反应中的催化性能

    The preparation of supported liquid-phase platinum catalyst, and its catalytic property for hydro-(silylation) reaction of 3-chloropropene were studied.

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  • 提出了苯基硅烷甲醇一步反应制得高效催化助剂DDS工艺

    A one-step process of synthesis of high-effective catalytic promotor DDS from diphenyldichlorosilane and methyl alcohol was put forward.

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  • 采用表面经过硅烷偶联剂原位修饰的纳米氧化增强橡胶

    A novel nano-silica surface-modified by silane was used as a reinforcing filler for HTV(heat vulcanization) silicone rubber.

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  • 列举常见的氧化化学改性方法,其改性主要有、有机化合物聚合物硅烷偶联

    General chemical modification methods were given. The general modifiers include alcohol, organosilicon compound, polymer and silane coupling agent.

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  • 本文主要是以乙酰氧基硅烷羧酸进行缩聚反应,合成一系列

    This paper reports the synthesis of a series of poly (silyl ester)s by diacetoxylsilane with several dicarboxylic acid.

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  • 考察温度催化剂用量加料速率等因素苯乙烯与甲基硅烷氢加成反应的影响。

    The effects of temperature, the quantity of catalyst used, and reactant feed rate on hydrosilylation was discussed.

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  • 纳米级氧化钛载体催化剂氢化硅烷化中的应用使用催化剂的氢化硅烷方法以及包括该催化剂的组合物。

    Platinum catalysts that are supported on nanoscale titanium dioxide, use thereof in hydrosilylation, hydrosilylation method using said catalysts and compositions comprising said catalysts.

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  • 自然放置正交实验考察苯基甲氧基硅烷稳定性

    The stability of dimethoxydiphenylsilane (DDS) in natural placement and orthogonal experiments was studied.

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  • 本文以研究硅烷氢化反应作为重点以期通过氢化反应解决茂铁衍生物作为催化剂固体推进剂中的迁移问题

    This thesis is focused on the hydrosilylation of ferrocenylsilanes, expecting to solve the problem of migration of ferrocene derivatives as combustion catalyst in solid propellant.

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  • 以正酸乙原料溶胶-凝胶过程制备氧化溶胶,再利用甲基乙氧硅烷DDS)对其进行改性,制备了疏水性氧化凝胶。

    Hydrophobic silica gel was prepared by sol-gel process using tetraethoxy silicone(TEOS) as raw material, then the surface was chemically modified by diethoxydimethylsilane(DDS).

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  • 研究甲基热解制备聚碳硅烷过程,探讨了合成条件产物特性影响

    Preparation of polycarbosilane (PCS) by pyrolysis of polydimethylsilane has been investigated. Effect of synthesis condition on the properties of products was studied.

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  • 溶胶— 凝胶法制薄膜,加入胶体氧化粒子硅烷控制薄膜表面粗糙度和表面化学性质。

    Super-hydrophobic silica-based thin films were prepared by sol-gel processing. Both surface energy and roughness were controlled using colloidal silica particles and fluoroalkylsilane.

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  • 实验研究直接法流化床合成甲基过程反应温度反应活性甲基硅烷(DDS)选择性影响

    The effect of reaction temperature on reaction activity and selectivity of dimethyl dichlorosilane (DDS) in direct synthesis process has been investigated experimentally.

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  • 甲基丙基一种重要有机中间体,采用甲基三乙氧基硅烷烯丙基通过格式反应制得。

    Diallylethoxylmethylsilane is an important silicone intermediate. It was prepared by reaction of methyltriethoxylsilane with allyl chloride grignard reagent.

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  • 本发明公开了一种色彩加深述色彩加深剂包含采用具有氨基偶联剂在酸性条件下处理氧化微粒聚醚改性的聚

    Disclosed is a color deepening agent containing silica particles which are treated with a silane coupling agent having an amino group under acidic conditions and a polyether-modified polysiloxane.

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  • 对多孔进行氧化硅烷化、抗体共价结合处理,制备出生物免疫传感器。

    The structure of immunosensor is prepared by the following steps: oxidization, silanization, glutaraldehyde cross-linker, and covalent binding of antibody.

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  • 单独收集三氯降低生产能耗避免级三氯氢原料硅烷之间交叉污染

    The single collection of the secondary trichlorosilane can reduce production energy consumption and avoid the cross contamination between the secondary trichlorosilane and raw chlorsilane.

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  • 讨论不同四甲氧基硅烷TMOS(PEG)配比老化条件、陈化时间胶柱影响采用SEM、BET强度测试等手段结构进行表征。

    The effects of TMOS/PEG ratios and aging conditions on the pore structure were investigated and the prepared samples were characterized by SEM, BET and hardness tester.

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  • 产物是双键经过重排的取代烯丙基甲基甲氧基硅烷6—10,该产物可进行一系列电取代反应

    The rearrangement of allylic double bond took placed in the course of these reaction. 6—12 are able to undergo a lot of electrophilic substitution reaction.

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  • 产物是双键经过重排的取代烯丙基甲基甲氧基硅烷6—10,该产物可进行一系列电取代反应

    The rearrangement of allylic double bond took placed in the course of these reaction. 6—12 are able to undergo a lot of electrophilic substitution reaction.

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