• 临界介质中2,6-二氟催化水解制备2,6-二氟苯甲酰胺方法

    Process of preparing 2,6-difluorobenzamide by 2.6-difluorobenz nitrile non catalyzing and hydrolyzing in near critical aqueous medium.

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  • 26 腈为原料,水解制得2 ,6 二氟苯甲酰胺,产率为92 % ;

    Difluorobenzamide was synthesized by fluorination and hydrolysis from 2,6 dichlobenil with the recovery of 92%.

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  • 二氟合成消炎镇痛氟苯水杨酸关键中间体

    Difluorobiphenyl is the key intermediate for the synthesis of antipyretic analgesic Diflunisal.

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  • 结果:尼美舒利增强硝基氟苯诱导迟发型变态反应,并且提高抗体水平增加脾脏重量

    Result: The severity of dinitrofluorobenzene-induced delay type of hypersensitivity was enhanced by nimesulide, the antibody level and weight of spleen were increased.

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  • 论还了2,4-氯-3,5-硝基三甲基合成方法影响收率反应温度,反应时间催化剂进行了研究。

    This paper reported the synthetic method of 2, 4-dichloro-3, 5-dinitrotrifluorotoluene. The effect of temperature, time, and catalyst on yield were studied.

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  • 本文采用相色谱HP-5毛细管,以甲酸物,用氢火焰离子化检测器对甲菊酯进行定性定量分析。

    A method for the determination of metofluthrin TC by GC with HP-5 capillary column, diisobutyl phthalate as internal standard and FID detector was described.

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  • 目的合成诺酮类抗菌药中间体甲酸,并改进工艺,使之适用于工业化生产。

    Objective To improve the synthesis of tetrafluorophthalic acid as an intermediate in preparing quinolone antibacterials.

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  • 说出来吓你,死尸会释放出二氟代甲烷等一系列奇怪化学物质。然而也正是这些物质帮助科学家找到各种隐秘墓穴

    Dead bodies emit a surprising array of chemicals, from benzene to freon, which can help forensic scientists find clandestine graves.

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  • 提出了一种以2,3-硝基原料,化、高温氯化、硝化、再化反应合成2,3,4-三硝基新工艺路线。

    A method is given for synthesis of 2,3,4 trifluoronitrobenzene from 2,3 dichloronitrobenzene by fluorination, chlorination, nitration, etc.

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  • 采用离子色谱同时测定合成药物中存在的四硼酸根、对甲基磺酸根、硫酸根、1,4-丁磺酸根4种离子。

    A new method of simultaneous separating and determining tetrafluoroborate, p-toluene sulphonic acid, sulfate radical and 1,4-Butanedisulfonie acid by ion chromatography was established.

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  • 目的探讨CD 8 +T细胞亚群尤其是CD 8 + CD2 8 - T抑制细胞2,4硝基氟苯(DNFB)大鼠实验性结肠炎模型中的变化及其可能作用。

    Objective To explore the changes of CD8 + t cell subtypes especially CD8 + CD28 -t suppressor cells in rats with experimental colitis induced by 2, 4-dinitrofluorobenzene (DNFB).

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  • 本文以邻甲基、对氯胺、间三甲基5-三甲基-1,3-单体,利用电化学方法,得到了上述衍生物的聚合物薄膜

    In this paper, polymer films were prepared with o-toluidine, p-chloroaniline, m-trifluoro methylaniline and 5-trifluoromethyl-1,3-diaminobenzene as monomer by electrochemical method.

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  • 方法:以4-氟苯甲酰环己酮、L-酪氨酸甲酯1,2-澳乙烷以及卡巴唑为原料,经3反应合成目标化合物。

    Methods:Chiglitazar was synthesized from 2-(4-fluoro)benzoylcyclohexanone, L-tyrosine methyl ester and 1,2-dibromoethane via 3 steps.

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  • 方法:以4-氟苯甲酰环己酮、L-酪氨酸甲酯1,2-澳乙烷以及卡巴唑为原料,经3反应合成目标化合物。

    Methods:Chiglitazar was synthesized from 2-(4-fluoro)benzoylcyclohexanone, L-tyrosine methyl ester and 1,2-dibromoethane via 3 steps.

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