结果用改良的薄层层析法分析多糖的单糖组成,得到清晰的图谱,与气相色谱法结果一致。
Results Distinct figures indicating the monosaccharide composition of polysaccharides obtained by the modified TLC were well consistent with those from GC method.
方法用不同的展开剂,采用薄层色谱法和纸层析法对全蝎抗凝活性成分进行鉴定和分析。
Methods Under the various separating condition, the anticoagulating active components of scorpion were appraised with thin layer chromatography(TLC) and paper chromatography.
采用薄层色谱法(TLC)确定柱层析的洗脱剂,并检测柱层析的分离效果,采用红外光谱法(IR)进行结构分析。
The eluant was selected by TLC and TLC was also used to identify the effect of the TLC separation, and the molecular constructures were characterized by IR.
用离子交换柱层析法分离,用反相高效液相色谱法进一步纯化,经聚丙烯酰胺凝胶电泳分析确定相对分子质量。
Methods The peptide was separated by ion exchange column chromatography and further purified by reverse phase HPLC, and the molecular weight was determined by tricine gel electro phoresis.
由离子色谱法和薄层层析法检测得知在此条件下寡聚半乳糖醛酸的产率大于54.3%,其中以二糖和三糖为主,产率分别为26.7%和27.6%;
The yield of the oligogalacturonic acid was more than 54.3%, mainly with a degree of polymerization (DP) 2 and 3, the yields of which were 26.7% and 27.6% respectively.
由离子色谱法和薄层层析法检测得知在此条件下寡聚半乳糖醛酸的产率大于54.3%,其中以二糖和三糖为主,产率分别为26.7%和27.6%;
The yield of the oligogalacturonic acid was more than 54.3%, mainly with a degree of polymerization (DP) 2 and 3, the yields of which were 26.7% and 27.6% respectively.
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