• 最后我们选用胺锂(LDA)为碱,在干冰酮浴下,合成磷酸很高的立体选择性。

    At last , we used the base: LDA, dry ice-acetone bath , to synthesize the enol phosphates and gain very high rigio-selectivity.

    youdao

  • 通过添加适量四丁基溴化转移催化剂使用过量的亚磷酸异丙补偿强碱环境中的水解,从而提高了反应产率

    The yield was increased through adding tetrabutyl ammonium bromide as the phase transfer catalyst, and using excessive diisopropyl phosphite to compensate its hydrolyzation.

    youdao

  • 通过添加适量四丁基溴化转移催化剂使用过量的亚磷酸异丙补偿强碱环境中的水解,从而提高了反应产率

    The yield was increased through adding tetrabutyl ammonium bromide as the phase transfer catalyst, and using excessive diisopropyl phosphite to compensate its hydrolyzation.

    youdao

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