方法:以2氨基4 ,5二甲氧基苯甲酸为原料,分别经过环化、氯代、取代等反应,合成了五种目标化合物。
The five quinazoline compounds were prepared by using 2 amino 4,5 dimethoxy benzoic acid as original material, which underwent ring closing, halogenation and substitution.
以二苯醚与苯甲酰氯为原料,合成了一种新型的激光光敏刺——4 -苯氧基二苯甲酮(PBZP)。
A new photoinitiator, 4-phenoxy benzophenone (PBZP), was synthesized and characterized using diphenyl ether and benzoyl chloride as raw material.
介绍了一种含环氧基聚酯的羟值测定方法,即乙酰氯法。
A method for determining hydroxyl value of epoxy-containing polyester, namely acetyl chloride method is introduced.
研究了以无水碳酸钠为催化剂,红霉素肟与甲氧基乙氧基氯甲醚(MEMC)为原料,一步合成罗红霉素的实验过程。
The experimental process on synthesis of roxithromycin was studied by using erythromycin oxime and MEMC as raw material under the catalytic action of anhydrous sodium carbonate.
着重研究5 -甲氧基吲哚、5 -甲基吲哚和5 -氯吲哚的稳定几何构型和分子中各原子上的电荷分布。
We mainly study stable molecular geometries and atomic charge distributing of 5-methoxy indole 5-methyl indole and 5-chlorin indole.
本课题以二茂铁为原料,与邻甲氧基苯甲酰氯反应生成邻甲氧基苯甲酰基二茂铁,再与一系列胺反应合成亚胺,最终还原为二茂铁氨基化合物。
The title compounds were obtained by the reduction of the corresponding ferrocenyl imines, which were prepared from ferrocene and o-anisic acid chloride, followed by amination with aromatic amines.
目的:探索4(2氯乙氧基)二苯酮的合成条件,包括原料配比、反应时间等。
Objective:In order to find the best condition for the synthesis of 4 (2 chloroethoxy)benzophenone, including the proportion of material, the time of reaction.
在三氯氧磷作用下,由芳氧基乙酸和氨基硫脲经脱水环合,微波辐射快速合成了一系列2氨基5芳氧亚甲基1,3,4噻二唑类化合物。
The reaction of aryloxy acetic acid with thiosemicarbazide in the presence of dehydrating agent, POCl_3, affords a series of 2amino5aryloxymethyl1,3,4thiadiazoles under microwave irradiation (MWI).
地克珠利、环丙氨嗪、莱克多巴胺、牛至香酚、氯氰碘柳胺钠、双乙酸钠、乙氧基喹啉、大蒜素、脲酶抑制剂。
Diclazuril, Cyromazine, Ethoxy Quinoline, Closantel Sodium, Ractopamine, Oregano Oil, Garlicin, Urease Inhibitor etc. raw material and 100 various products such as preparation.
目的建立溴芬酸钠原料中二氯甲烷、甲苯、1,2-二甲氧基乙烷、乙酸乙酯、乙醇残留量测定方法。
Objective To establish a method for detection of dichloromethane, 1,2-dimethoxyethane, toluene, ethyl acetate and ethanol in bromfenac sodium.
甲基二烯丙基硅烷是一种重要的有机硅中间体,采用甲基三乙氧基硅烷和烯丙基氯通过格式反应制得。
Diallylethoxylmethylsilane is an important silicone intermediate. It was prepared by reaction of methyltriethoxylsilane with allyl chloride grignard reagent.
为解决胶原酶免疫原性,采用经氯甲酸对硝基苯酯活化的单甲氧基聚乙二醇来修饰胶原酶。
In order to overcome the immunogenicity of collagenase, the enzyme was modified with monomethoxypolyethylene glycol 5000 (mPEG) activated by p nitrophenyl chloroformate.
用苯酚和钠得到苯酚钠,苯酚钠和2-氯乙醇得到2-苯氧基乙醇,与氯化锌反应得2,3-二氢苯并呋喃,产率50%。
A mixture of phenol, sodium and 2-chloroethanol forms 2-phenoxyethanol, add zinc chloride, the product is 2,3-dihydrobenzofuran, yield 50%.
以苯酚、环氧氯丙烷为原料,KOH为催化剂,肼解后合成了1—氨基—3—苯氧基—2—丙醇。
The 1-amino-3-phenoxyl-2-propanol is prepared with phenol and epoxy chloropropane by means of KOH as catalyst and hydrazinolysis.
本文报道通过亚稳离子和精确质量测定,讨论了1,1—二氯—2—乙氧基—2—芳基烯烃的质谱裂解规律。
A study on the mass spectrometric cleavage of 1, 1—dichloro—2—ethyloxy—2—AryIolefins by metastable ions and precise mass measurement is reported.
反应混合物可以进一步酯化重排制备维生素A的中间体1-氯-2-甲基-4-乙酰氧基-2-丁烯。
The reaction mixture then undergo esterification and rearrangement reaction to prepare 1-chloro-2-methyl-4-(acetyloxy)-2-butene, which is a important intermediate of vitamin A.
公司主要产品为烷氧基硅烷、盐酸、沉淀法白炭黑、三氯氢硅、有机硅精细化学品等。
Our main products are alkoxy silanes, hydrochloric acid, trichlorosilane, Precipitated silica, fine chemicals of organosilicon.
以对甲氧基苯甲醛、三氯甲烷为原料,相转移催化羰基加成法合成了对甲氧基苯乙醇酸。
Based on the principle of phase transfer catalysis, 4-methoxy-phenylhydroxy-acetic acid was synthesized by the carbonyl addition reaction of 4-methoxybenzaldehyde.
前言:以邻苯二酚和二氯甲烷为原料,二甲亚砜为溶剂,在碱性条件下合成1,2-亚甲二氧基苯,产品收率达到73.4%;
2-(methylenedioxy)benzene is synthesized by using catechol, dichloromethane and dimethylsulfoxide with the condition of alkali and normal pressure. Overall yield of the process is 73.4%.
以邻甲氧基苯酚与对氯*为原料,经四步反应合成6-(2-甲氧苯氧基)-1,4-二氢-4-氧代-3-喹啉羧酸乙酯。经抗鸡球虫实验证明具有抗球虫效果。
The compound 6-(2-methoxy phenoxy)-1, 4-dihydrogen-4-oxo-3-ethyl quinoline carboxylate is prepared with o-methoxyphenol and p-chloronitrobenzene as materials and through four-step reaction.
以邻甲氧基苯酚与对氯*为原料,经四步反应合成6-(2-甲氧苯氧基)-1,4-二氢-4-氧代-3-喹啉羧酸乙酯。经抗鸡球虫实验证明具有抗球虫效果。
The compound 6-(2-methoxy phenoxy)-1, 4-dihydrogen-4-oxo-3-ethyl quinoline carboxylate is prepared with o-methoxyphenol and p-chloronitrobenzene as materials and through four-step reaction.
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