其中,乙醇作为氢氧化锆沉淀洗涤介质时,可以有效地消除粉末团聚颗粒。
Especially after washing the precipitation using ethanol, there are almost no agglomerate particles.
以H_2SO_4处理四甲基氯化铵的有机溶液,立即生成沉淀,经过滤、洗涤、干燥后,得到白色结晶状固体——TMAHS。
To treat tetramethyl ammonium chloride with H2SO4 in organic solvent, a precipitate is produced. A white crystallizing solid TMAHS is prepared after filtrating, washing and drying.
反应产物用稀盐酸溶液洗涤,将所得沉淀干燥后经分离纯化,对纯化产物进行高分辨质谱、红外光谱鉴定。
The residue was washed with dilute hydrochloric acid solution, The precipitation was dried, purified, and identified by the infrared spectrometry (IR) and high mass spectrometry(HRMS)with DES-HS.
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