本课题以二茂铁为原料,与邻甲氧基苯甲酰氯反应生成邻甲氧基苯甲酰基二茂铁,再与一系列胺反应合成亚胺,最终还原为二茂铁氨基化合物。
The title compounds were obtained by the reduction of the corresponding ferrocenyl imines, which were prepared from ferrocene and o-anisic acid chloride, followed by amination with aromatic amines.
传统的肽类合成多采用液相化学合成,常用的包括碳二亚胺法,混合酸酐法、酰氯法、叠氮物法等等,为多肽的合成提供了多种选择。
Peptides are traditionally synthesized in liquid phase, such methods are DCC, mixed anhydrides, acyl chloride and azide etc. , which provide more choices for peptides synthesis.
本文用2-氯-5-氯甲基吡啶经氨基化,和N-氰基乙亚胺酸乙酯反应,最后甲基化得到吡虫清。
In this thesis, 2-chloro-5-chloromethyl pyridine is ammoniated, which followed by the reaction with N-cyano ethyl ethylimidoate, finally is methylated to gain the objective product.
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