In step (C), a 300-gallon reaCtion vessel was Charged with 300 kg of phosphorus oxyChloride (6), Cooled, and blanketed with nitrogen.
步骤(c),往300加仑的反应容器里加入300千克三氯氧化磷(6),冷却,并覆以氮气。
Some technological conditions of the synthesis of triphenyl phosphate by the reaction of sodium phenolate and phosphorus oxychloride were studied, and a better process was found out.
研究了常温下由苯酚钠悬胶体与三氯氧磷反应合成磷酸三苯酯的工艺条件,找到了一条比较好的合成方法。
A synthetic method of direct cyclization was researched that 2-chloro-2-chloromethyl-4-cyanobutyraldehyde was reacted with phosphorus oxychloride to get 2-chloro-5-chloromethylpyridine.
研究了一种直接环合的方法,用2-氯-2氯甲基- 4- 氰基丁醛与三氯氧磷反应来制备2-氯-5-氯甲基吡啶。
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